Flavin-catalyzed aerobic oxidation of sulfides and thiols with formic acid/triethylamine.

نویسندگان

  • Shun-Ichi Murahashi
  • Dazhi Zhang
  • Hiroki Iida
  • Toshio Miyawaki
  • Masaaki Uenaka
  • Kenji Murano
  • Kanji Meguro
چکیده

An efficient and practical catalytic method for the aerobic oxidative transformation of sulfides into sulfoxides, and thiols into disulfides with formic acid/TEA in the presence of a new, readily available, and stable flavin catalyst 5d is described.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Cellulose Sulfuric Acid: As an Efficient Bio Polymer Based Catalyst for the Selective Oxidation of Sulfides and Thiols by Hydrogen Peroxide

Cellulose sulfuric acid as a bio-polymer based solid catalyst efficiently catalyzes the selectively oxidation of sulfides to sulfoxides and thiols to disulfides using hydrogen peroxide as a green oxidant with good yields at room temperature. The developed method offers a number of advantages such as high selectivity, mild reaction conditions, simple operation, cleaner reaction profiles, low...

متن کامل

Efficient oxidation of sulfides using a molybdenum(VI)–dioxo complex containing an benzimidazole ligand

For the first time, dioxomolybdenum(VI) complex with the general formula [MoO2L2] containing a N-O bidentate ligands (HL=2-(o-aminophenyl)- benzimidazole) has been used for the oxidation of sulfides. Elemental analyses (carbon, hydrogen, nitrogen), FT-IR and Uv-Visble spectra and 1HNMR analysis agree well with the proposed stoicheiometry of the complex [MoO...

متن کامل

Tertiary amine mediated aerobic oxidation of sulfides into sulfoxides by visible-light photoredox catalysis on TiO2.

The selective oxidation of sulfides into sulfoxides receives much attention due to industrial and biological applications. However, the realization of this reaction with molecular oxygen at room temperature, which is of importance towards green and sustainable chemistry, remains challenging. Herein, we develop a strategy to achieve the aerobic oxidation of sulfides into sulfoxides by exploring ...

متن کامل

Multi-wall Carbon Nanotubes Supported Molybdenum Acetylacetonate: Efficient and Highly Reusable Catalysts for Oxidation of Sulfides with Tert-butyl Hydroperoxide

In the present work, highly efficient oxidation of sulfides catalyzed by MoO2(acac)2 supported on multi-wall carbon nanotubes, MWCNTs, modified with 1,2-diaminobenzene (DAB) and 2-aminophenol (AP), at room temperature are reported. The effects of various parameters such as reaction time, solvent, catalyst amount, oxidant, etc, were studied. These heterogenized catalysts showed high activity in ...

متن کامل

Efficient recyclable CuI-nanoparticle-catalyzed S-arylation of thiols with aryl halides on water under mild conditions.

CuI nanoparticles efficiently catalyzed the C-S cross coupling of aryl and alkyl thiols with aryl halides in the absence of ligands on water under mild conditions. A wide range of diaryl sulfides and aryl alkyl sulfides are synthesized in good to excellent yields utilizing this protocol. This procedure is particularly noteworthy given its mild conditions, avoiding the undesired formation of dis...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Chemical communications

دوره 50 71  شماره 

صفحات  -

تاریخ انتشار 2014